Problem developing plates

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  • #7652
    Krokodul
    Participant

    Hi all,

    I’ve run into a new problem that hopefully someone can shed some light on. My latest few plates all have really big image particles and droplets of mercury in the shadow areas. I can’t seem to remedy this problem. I cut my developing time to 2 1/2 minutes at 90°C and also tried lowering the temperature of my mercury bath to 70°C but it didn’t really make a difference. I feel a bit lost, and was wondering if you guys could help me understand what’s going on? I’ve attached a photo showing the Daguerreotype through a jeweler’s loupe.

    Daniel

    plate1.jpg

    plate2.jpg

    #11072
    CasedImage
    Keymaster

    Your development time is too hot and too quick, try extending your development time as well as dropping your temp to 70 deg C, you need to find a point of development time/temp for the sensitization and exposure of your plates that doesn’t rely on over development. Nice looking plates otherwise, congrats.

    www.CasedImage.com

    #9809
    Pobboravsky
    Participant

    Hi Daniel and Alan,

    The proper dev’g time-temperature depends to some extent upon the design of the mercurizer. Early on, when I was working with quarter-plates I successfully dev’d at 90 deg. C for 75 seconds without frosting in the shadows.

    In 1989, when Grant Romer and I made d-types in Paris we developed 5×7-inch plates for 6 or 7 minutes at 80 deg. C. This was done with a mercurizer of a different design.

    However, either one of the above two Time-Temps. is a good starting point for your dev’g box, Daniel.

    For the benefit of those starting out it would be interesting to list the good time-temp used by workers.

    Good luck,

    Irv

    #9811
    Krokodul
    Participant

    Hi Alan and Irv,

    I really appreciate your suggestions. Thank you very much! So this it what mercury frosting looks like? The weird thing is that the problem started only recently. I developed several plates for 3 minutes at 90 deg. C without frosting before. I suppose it could be because I changed the concentration of my bromine water? There’s another question that’s been bugging me: Do you try to keep the temperature constant during development or do you turn off the heat once the mercury reaches the desired temperature? I’m using a small alcohol lamp that I put out as soon the pot is up to temperature.

    Thanks again,

    Daniel

    #9813
    Pobboravsky
    Participant

    Some of the 19th century daguerreian literature mentions putting out the flame of the alcohol lamp once the mercury reaches the aim temperature. I have no experience doing that. However, continue to do that; you don’t want to change in mid stream. Mike Robinson jokes that if you get good results while wearing green socks, wear them every time you make daguerreotypes.

    The time-temperature values I gave assume that the thermometer is measuring the temp. of the mercury itself.

    Good luck,

    Irv

    In my experience wearing brown socks always ends in failure.

    #10146
    newone2010
    Participant

    I meet same questions now.As my English is so poor,I always understand what you mentioned with mistakes.So I always made mistakes in making dags.

    The mercury time:

    Does it depend on devloping time/temprature and the balance of Br-I?

    Different balance of Br-I needs different Mercury time?

    Looking forward for your reply.

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